Course Description
| Course | Code | Semester | T+P (Hour) | Credit | ECTS |
|---|---|---|---|---|---|
| PHARMACEUTICAL CHEMISTRY LAB. IV | - | Spring Semester | 0+3 | 1,5 | 3 |
| Course Program |
| Prerequisites Courses | |
| Recommended Elective Courses |
| Language of Course | Turkish |
| Course Level | First Cycle (Bachelor's Degree) |
| Course Type | Required |
| Course Coordinator | Prof.Dr. Seda ÜNSALAN |
| Name of Lecturer(s) | Assist.Prof. Hacer KARATAŞ BRISTOW |
| Assistant(s) | |
| Aim | The aims of this course to give information on qualitative analysis of pharmaceutical active compounds and to make the application. |
| Course Content | This course contains; 1. Qualitative analysis of active compound(general concepts),2. Determination of the physical properties and the elements,3. Determination of the functional group.,4. Specific reactions,5. specific reactions,6. analysis of unknown samples.,7. analysis of unknown samples,8. analysis of unknown samples,9. analysis of unknown samples,10 NMR spectroscopic methods,11 NMR spectroscopic methods,12 MS Spectroscopic Methods,13 UV. Vis., IR, NMR and MS spectral data solution,14 UV. Vis., IR, NMR and MS spectral data solution. |
| Dersin Öğrenme Kazanımları | Teaching Methods | Assessment Methods |
| 1. adapt the analysis methods of pharmaceutical active substances. | 12, 14, 17, 9 | A, D |
| 1.1. determine the physical properties of the drugs. | 12, 14, 17, 9 | A, D |
| 1.2. determine the elemental analysis of the drugs. | 12, 14, 17, 9 | A, D |
| 1.3. determine of functionalgroups of the drugs. | 12, 14, 17, 9 | A, D |
| 1.4. arrange specific reactions of the drugs. | 12, 14, 17, 9 | A, D |
| 2. will be able to analyse the NMR spectra. | 12, 14, 17, 9 | A, D |
| 2.1. interpret the chemical schift in NMR. | 12, 14, 17, 9 | A, D |
| 2.2. use the NMR data in druganalysis. | 12, 14, 17, 9 | A, D |
| 2.3. evaluate the NMR spectra of synthesized compounds. | 12, 14, 17, 9 | A, D |
| 3. analyse the MS spectra. | 12, 14, 17, 9 | A, D |
| 3.1. interpret the MS fragmentation patterns. | 12, 14, 17, 9 | A, D |
| 3.2. use the MS data in drug analysis. | 12, 14, 17, 9 | A, D |
| 3.3. evaluate the MS spectra of synthesized compounds. | 12, 14, 17, 9 | A, D |
| 4. relate the UV. - Vis., IR, NMR and MS spektral techniques. | 12, 14, 17, 9 | A, D |
| 4.1. interpret UV. Vis., IR, NMR and MS spectral data. | 12, 14, 17, 9 | A, D |
| 4.2. interpret the UV. Vis., IR, NMR and MS spectral data of the drugs. | 12, 14, 17, 9 | A, D |
| Teaching Methods: | 12: Problem Solving Method, 14: Self Study Method, 17: Experimental Technique, 9: Lecture Method |
| Assessment Methods: | A: Traditional Written Exam, D: Oral Exam |
Course Outline
| Order | Subjects | Preliminary Work |
|---|---|---|
| 1 | 1. Qualitative analysis of active compound(general concepts) | 1 |
| 2 | 2. Determination of the physical properties and the elements | 1 |
| 3 | 3. Determination of the functional group. | 1 |
| 4 | 4. Specific reactions | 1 |
| 5 | 5. specific reactions | 1 |
| 6 | 6. analysis of unknown samples. | 1 |
| 7 | 7. analysis of unknown samples | 1 |
| 8 | 8. analysis of unknown samples | 1 |
| 9 | 9. analysis of unknown samples | 1 |
| 10 | 10 NMR spectroscopic methods | 1 |
| 11 | 11 NMR spectroscopic methods | 1 |
| 12 | 12 MS Spectroscopic Methods | 1 |
| 13 | 13 UV. Vis., IR, NMR and MS spectral data solution | 1 |
| 14 | 14 UV. Vis., IR, NMR and MS spectral data solution | 1 |
| Resources |
| 1. The laboratory notes will be given to the students. |
Course Contribution to Program Qualifications
| Course Contribution to Program Qualifications | |||||||
| No | Program Qualification | Contribution Level | |||||
| 1 | 2 | 3 | 4 | 5 | |||
| 1 | PQ-1. Skilfully use information technology to access, follow, evaluate and apply current knowledge in the field of Pharmaceutical Sciences. | X | |||||
| 2 | PQ-2. Have advanced knowledge in APIs and DPs. | X | |||||
| 3 | PQ-3. Collaborate with the experts for collection, interpretation, application and declaration of data in Pharmaceutical Sciences field. | X | |||||
| 4 | PQ-4. Provide best patient counseling services and medication therapy management using his/her knowledge and pharmaceutical information systems to improve the quality of life and safety of patient. | X | |||||
| 5 | PQ-5. Capable of organizing and administering a drugstore as per responsibilities prescribed under the Pharmacy Law, using skills, knowledge and advanced technology systems. | X | |||||
| 6 | PQ-6. Skilfully use computer programs and advanced technology related to the Pharmaceutical Sciences. | X | |||||
| 7 | PQ-7. Provide solutions to the professional issues using scientific knowledge and data. | X | |||||
| 8 | PQ-8. Perform identification, quality control and standardization of the drug products. | X | |||||
| 9 | PQ-9. Prepare and implement developmental plans for his/her subordinates, frequently evaluate their progress and make necessary adjustments. | X | |||||
| 10 | PQ-10. Capable of conducting independent studies with his/her advanced knowledge in pharmaceutical sciences, takes responsibilities in professional organizations and efficiently collaborates with the members of his/her own organization as well as other organizations. | X | |||||
| 11 | PQ-11. Clearly show signs of adoption of life-long learning and openness to further development. | X | |||||
| 12 | PQ-12. Critically evaluate their knowledge in pharmaceutical sciences. | X | |||||
| 13 | PQ-13. Closely follow and evaluate the national and international professional developments. | X | |||||
| 14 | PQ-14. Record and document all professional activities and applications. | X | |||||
| 15 | PQ-15. Communicate all necessary information about medicines to patient, medical personnel and public. | X | |||||
| 16 | PQ-16. Proficient in English to communicate and follow current knowledge in pharmaceutical sciences. | X | |||||
| 17 | PQ-17. Inform officials and organizations about the issues with the quality assurance of pharmaceutical products. | ||||||
| 18 | PQ-18. Actively involve in the preparation of APIs, every stage of the formulation and production of DPs. | X | |||||
| 19 | PQ-19. Knowledgable in the regulatory rules of new drug application, data protection and patent issues and understand their interrelationship. | X | |||||
| 20 | PQ-20. Have awareness of his/her duties, rights and responsibilities and act based on Pharmacy Law and high professional ethical standards. | X | |||||
| 21 | PQ-21. Familiar with and actively pursue the personal and public health, environmental, and work safety issues. | X | |||||
Assessment Methods
| Contribution Level | Absolute Evaluation | |
| Rate of Midterm Exam to Success | 60 | |
| Rate of Final Exam to Success | 40 | |
| Total | 100 | |
| ECTS / Workload Table | ||||||
| Activities | Number of | Duration(Hour) | Total Workload(Hour) | |||
| Course Hours | 14 | 3 | 42 | |||
| Guided Problem Solving | 14 | 3 | 42 | |||
| Resolution of Homework Problems and Submission as a Report | 0 | 0 | 0 | |||
| Term Project | 0 | 0 | 0 | |||
| Presentation of Project / Seminar | 0 | 0 | 0 | |||
| Quiz | 0 | 0 | 0 | |||
| Midterm Exam | 1 | 3 | 3 | |||
| General Exam | 1 | 3 | 3 | |||
| Performance Task, Maintenance Plan | 0 | 0 | 0 | |||
| Total Workload(Hour) | 90 | |||||
| Dersin AKTS Kredisi = Toplam İş Yükü (Saat)/30*=(90/30) | 3 | |||||
| ECTS of the course: 30 hours of work is counted as 1 ECTS credit. | ||||||
Detail Informations of the Course
Course Description
| Course | Code | Semester | T+P (Hour) | Credit | ECTS |
|---|---|---|---|---|---|
| PHARMACEUTICAL CHEMISTRY LAB. IV | - | Spring Semester | 0+3 | 1,5 | 3 |
| Course Program |
| Prerequisites Courses | |
| Recommended Elective Courses |
| Language of Course | Turkish |
| Course Level | First Cycle (Bachelor's Degree) |
| Course Type | Required |
| Course Coordinator | Prof.Dr. Seda ÜNSALAN |
| Name of Lecturer(s) | Assist.Prof. Hacer KARATAŞ BRISTOW |
| Assistant(s) | |
| Aim | The aims of this course to give information on qualitative analysis of pharmaceutical active compounds and to make the application. |
| Course Content | This course contains; 1. Qualitative analysis of active compound(general concepts),2. Determination of the physical properties and the elements,3. Determination of the functional group.,4. Specific reactions,5. specific reactions,6. analysis of unknown samples.,7. analysis of unknown samples,8. analysis of unknown samples,9. analysis of unknown samples,10 NMR spectroscopic methods,11 NMR spectroscopic methods,12 MS Spectroscopic Methods,13 UV. Vis., IR, NMR and MS spectral data solution,14 UV. Vis., IR, NMR and MS spectral data solution. |
| Dersin Öğrenme Kazanımları | Teaching Methods | Assessment Methods |
| 1. adapt the analysis methods of pharmaceutical active substances. | 12, 14, 17, 9 | A, D |
| 1.1. determine the physical properties of the drugs. | 12, 14, 17, 9 | A, D |
| 1.2. determine the elemental analysis of the drugs. | 12, 14, 17, 9 | A, D |
| 1.3. determine of functionalgroups of the drugs. | 12, 14, 17, 9 | A, D |
| 1.4. arrange specific reactions of the drugs. | 12, 14, 17, 9 | A, D |
| 2. will be able to analyse the NMR spectra. | 12, 14, 17, 9 | A, D |
| 2.1. interpret the chemical schift in NMR. | 12, 14, 17, 9 | A, D |
| 2.2. use the NMR data in druganalysis. | 12, 14, 17, 9 | A, D |
| 2.3. evaluate the NMR spectra of synthesized compounds. | 12, 14, 17, 9 | A, D |
| 3. analyse the MS spectra. | 12, 14, 17, 9 | A, D |
| 3.1. interpret the MS fragmentation patterns. | 12, 14, 17, 9 | A, D |
| 3.2. use the MS data in drug analysis. | 12, 14, 17, 9 | A, D |
| 3.3. evaluate the MS spectra of synthesized compounds. | 12, 14, 17, 9 | A, D |
| 4. relate the UV. - Vis., IR, NMR and MS spektral techniques. | 12, 14, 17, 9 | A, D |
| 4.1. interpret UV. Vis., IR, NMR and MS spectral data. | 12, 14, 17, 9 | A, D |
| 4.2. interpret the UV. Vis., IR, NMR and MS spectral data of the drugs. | 12, 14, 17, 9 | A, D |
| Teaching Methods: | 12: Problem Solving Method, 14: Self Study Method, 17: Experimental Technique, 9: Lecture Method |
| Assessment Methods: | A: Traditional Written Exam, D: Oral Exam |
Course Outline
| Order | Subjects | Preliminary Work |
|---|---|---|
| 1 | 1. Qualitative analysis of active compound(general concepts) | 1 |
| 2 | 2. Determination of the physical properties and the elements | 1 |
| 3 | 3. Determination of the functional group. | 1 |
| 4 | 4. Specific reactions | 1 |
| 5 | 5. specific reactions | 1 |
| 6 | 6. analysis of unknown samples. | 1 |
| 7 | 7. analysis of unknown samples | 1 |
| 8 | 8. analysis of unknown samples | 1 |
| 9 | 9. analysis of unknown samples | 1 |
| 10 | 10 NMR spectroscopic methods | 1 |
| 11 | 11 NMR spectroscopic methods | 1 |
| 12 | 12 MS Spectroscopic Methods | 1 |
| 13 | 13 UV. Vis., IR, NMR and MS spectral data solution | 1 |
| 14 | 14 UV. Vis., IR, NMR and MS spectral data solution | 1 |
| Resources |
| 1. The laboratory notes will be given to the students. |
Course Contribution to Program Qualifications
| Course Contribution to Program Qualifications | |||||||
| No | Program Qualification | Contribution Level | |||||
| 1 | 2 | 3 | 4 | 5 | |||
| 1 | PQ-1. Skilfully use information technology to access, follow, evaluate and apply current knowledge in the field of Pharmaceutical Sciences. | X | |||||
| 2 | PQ-2. Have advanced knowledge in APIs and DPs. | X | |||||
| 3 | PQ-3. Collaborate with the experts for collection, interpretation, application and declaration of data in Pharmaceutical Sciences field. | X | |||||
| 4 | PQ-4. Provide best patient counseling services and medication therapy management using his/her knowledge and pharmaceutical information systems to improve the quality of life and safety of patient. | X | |||||
| 5 | PQ-5. Capable of organizing and administering a drugstore as per responsibilities prescribed under the Pharmacy Law, using skills, knowledge and advanced technology systems. | X | |||||
| 6 | PQ-6. Skilfully use computer programs and advanced technology related to the Pharmaceutical Sciences. | X | |||||
| 7 | PQ-7. Provide solutions to the professional issues using scientific knowledge and data. | X | |||||
| 8 | PQ-8. Perform identification, quality control and standardization of the drug products. | X | |||||
| 9 | PQ-9. Prepare and implement developmental plans for his/her subordinates, frequently evaluate their progress and make necessary adjustments. | X | |||||
| 10 | PQ-10. Capable of conducting independent studies with his/her advanced knowledge in pharmaceutical sciences, takes responsibilities in professional organizations and efficiently collaborates with the members of his/her own organization as well as other organizations. | X | |||||
| 11 | PQ-11. Clearly show signs of adoption of life-long learning and openness to further development. | X | |||||
| 12 | PQ-12. Critically evaluate their knowledge in pharmaceutical sciences. | X | |||||
| 13 | PQ-13. Closely follow and evaluate the national and international professional developments. | X | |||||
| 14 | PQ-14. Record and document all professional activities and applications. | X | |||||
| 15 | PQ-15. Communicate all necessary information about medicines to patient, medical personnel and public. | X | |||||
| 16 | PQ-16. Proficient in English to communicate and follow current knowledge in pharmaceutical sciences. | X | |||||
| 17 | PQ-17. Inform officials and organizations about the issues with the quality assurance of pharmaceutical products. | ||||||
| 18 | PQ-18. Actively involve in the preparation of APIs, every stage of the formulation and production of DPs. | X | |||||
| 19 | PQ-19. Knowledgable in the regulatory rules of new drug application, data protection and patent issues and understand their interrelationship. | X | |||||
| 20 | PQ-20. Have awareness of his/her duties, rights and responsibilities and act based on Pharmacy Law and high professional ethical standards. | X | |||||
| 21 | PQ-21. Familiar with and actively pursue the personal and public health, environmental, and work safety issues. | X | |||||
Assessment Methods
| Contribution Level | Absolute Evaluation | |
| Rate of Midterm Exam to Success | 60 | |
| Rate of Final Exam to Success | 40 | |
| Total | 100 | |